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Ball Milling In Inert Atmosphere

Ball Milling In Inert Atmosphere

The solutionbased reaction in dry THF and under nitrogen atmosphere at 50 176C with either zinc flakes or granular zinc no additive used resulted in low yields of 7 and 4, respectively Scheme 4 B, whereas under ballmilling conditions without any solvent, inert gas, or additive Table 2, the reaction proceeded smoothly in 2 h and all.

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